home  /  materials & metallurgical
department of materials & metallurgical

Materials & metallurgical failure analysis.

Corrosion, fatigue, fracture, hydrogen, and welding failures all leave a physical record in the metal itself. We read it — independently, and to a standard that holds up in court.

get started

What failed?

Start a conversation with our AI Research Concierge, already scoped to materials & metallurgical. Select a specialization to prompt it, or describe your situation directly.

AI Research Conciergematerials & metallurgical · triage, not a substitute for an expert
Tell me what failed and I'll help scope it — the likely mechanisms, what to preserve, and which expert fits. I won't give the formal analysis here.

Metals fail by a limited number of well-understood mechanisms, and each one leaves a signature that survives the event: striations on a fatigue fracture, branching cracks from stress-corrosion, a pit with an acidified interior, a hydrogen-embrittled bolt that sheared with almost no plastic deformation. The physics is not in dispute — what is in dispute is which mechanism actually operated on this part, under these loads, in this environment, and whether the material, the design, or the process is responsible. This department covers the failure modes where metallurgy decides the outcome, from a corroding buried pipeline to a cracked weld to a fastener that let go without warning.

specialization areas

Specialization areas in this department.

Each specialization area covers a distinct failure mechanism with its own physics, examination protocol, and governing standards. Start with the one that matches your incident.

methodology

How this department investigates.

Materials investigations move from the macro scale to the microstructure, preserving fracture and corrosion evidence at every step so nothing is lost before it can be examined.

MetallographySectioning, mounting, and polishing to reveal microstructure, grain boundaries, and crack morphology at the site of failure.
SEM / EDS fractographyHigh-magnification imaging and elemental analysis of fracture surfaces, corrosion products, and deposits.
Mechanical property testingHardness, tensile, impact, and fracture-toughness testing verified against the design and material specification.
Chemical composition analysisOES and XRF to confirm alloy identity and composition against the specified grade.
Non-destructive testingUltrasonic, radiographic, magnetic-particle, and dye-penetrant inspection to map defects without destroying evidence.
Standards & spec compliance reviewMaterial certifications, fabrication records, and inspection history against the governing codes and standards.
news & insights

News & insights from this department.

Technical briefings and case analyses on corrosion, fracture, and welding failures — written by the people who investigate them.

What wire-brushing a corroded pipe destroys

In a corrosion failure the scale and deposits are not debris covering the evidence. They are the evidence. Blasting, brushing or acid descaling before examination removes the record of the mechanism.

read

Was it the alloy or the environment it was put in?

Galvanic couples, area ratios, coating breaches, deposits and biofilms all accelerate corrosion locally. Each points at a different decision — material selection, coating spec, or how the asset was run.

read

Average wall loss and the single pit problem

General corrosion is an allowance and inspection question. Pitting and crevice attack perforate a wall the average calls healthy — and the two are measured, rated and reported by different rules.

read

Rated fatigue life against the actual duty cycle

A part that fails before its rated life is a claim about loading assumptions as much as about metal. How high-cycle, low-cycle, corrosion and thermal fatigue relate to a stated design life.

read

Dating a crack from what the fracture surface recorded

Beach marks record interruptions in service; striations record individual cycles. Both are evidence of a crack's history, and both are routinely overread. What a fatigue fracture surface can and cannot date.

read

Crack initiation is where the answer usually is

Most of a fatigue life is spent starting the crack, not growing it. That makes the initiation site — a machining mark, an inclusion, a pit, a fretting scar — the part of the fracture that holds the answer.

read
all materials & metallurgical insights
common questions

Materials & metallurgical failure analysis — the questions we hear.

How do you determine which failure mechanism actually occurred?

Each mechanism — fatigue, corrosion, hydrogen embrittlement, stress-corrosion cracking, overload — leaves a distinct signature on the fracture surface and in the microstructure. We start with low-magnification fractography to orient the failure, then move to SEM and metallography to confirm or rule out specific mechanisms. The conclusion is drawn from what the metal shows, not from the sequence of events as reported.

Can you tell whether this was a material defect, a design issue, or an operating condition?

Usually, yes. Material and process defects tend to be intrinsic — an inclusion, an out-of-spec composition, an improper heat treatment — and are found by comparing the failed part against its own certification and against unused stock. Design and operating issues show up as stress, environment, or loading conditions inconsistent with the part rating. Separating the two is largely what determines liability.

What parts or samples do you need for the analysis?

The failed component itself, wherever possible, plus an exemplar or unused unit for comparison, and any material certifications, drawings, or maintenance records available. For corrosion and cracking investigations, samples of the environment — water, soil, process fluid, deposits — are often just as important as the metal.

Which standards govern these investigations?

It depends on the mechanism and industry. ASTM standards govern most material testing (E8 tensile, E23 Charpy impact, E399 fracture toughness, E1820 J-integral, the G-series corrosion tests). NACE/AMPP standards (MR0175/ISO 15156, SP0169) govern corrosion and cracking in oil-and-gas and cathodic-protection service. AWS D1.1 and ASME Section IX govern welding. ASME B31 and Section VIII govern pressure-equipment fitness-for-service.

Something metal failed. Find out why.

Describe the incident. We will scope it and connect you with the right expert — usually within one business day.

failure-analysis assistanttriage · not a substitute for an expert
Tell me what failed and I'll help scope it — the likely mechanisms, what to preserve, and which expert fits. I won't give the formal analysis here.